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post lab 8 questions, Assignments of Chemistry

Questions for post lab 8 organic chemistry

Typology: Assignments

2023/2024

Uploaded on 06/13/2024

sadgirl69
sadgirl69 🇺🇸

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Experiment 8: Preparation of Adipic Acid from Cyclohexene
Exp 8-1
Name: ____________________________
(2 pts) _____1. Turned in on time
(19 pts) _____2. Header for all pages
POST LAB QUESTIONS:
1. Why do we add methanol to the reaction if we see a purple ring on the filter paper?
2. What reaction is occurring with the methanol (show reaction)? Does this reaction affect
your product?
3. Why do you get a precipitate when adding the HCl to make the solution acidic?
4. Calculate the theoretical yield for this reaction using measurements from procedure.
5. If you obtained an actual yield of 0.57g, what is the % yield?
6. What IR absorptions do you expect for the starting material (only in the functional group
region 4000cm-1 to 1500cm-1)?
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Experiment 8: Preparation of Adipic Acid from Cyclohexene

Exp 8-

Name: ____________________________

(2 pts) _____1. Turned in on time

(19 pts) _____2. Header for all pages

POST LAB QUESTIONS:

1. Why do we add methanol to the reaction if we see a purple ring on the filter paper?

2. What reaction is occurring with the methanol (show reaction)? Does this reaction affect

your product?

3. Why do you get a precipitate when adding the HCl to make the solution acidic?

4. Calculate the theoretical yield for this reaction using measurements from procedure.

5. If you obtained an actual yield of 0.57g, what is the % yield?

6. What IR absorptions do you expect for the starting material (only in the functional group

region 4000cm

to 1500cm

Experiment 8: Preparation of Adipic Acid from Cyclohexene

Exp 8-

7. What IR absorptions do you expect for the product (only in the functional group region

4000cm

to 1500cm

8. If you performed this lab, what should you get for the products melting point? _______

10. Complete the following reactions:

KMnO

4

MnO

2

H

2

+ O

KOH

KMnO 4

MnO 2

H

2

+ O

KOH

KMnO

4

MnO

2

H

2

O

+ KOH

O

OH

HO

O